Information card for entry 7120735

Structure parameters

• Chemical name: Sb12Zn4 cluster
• Formula: C76.55 H146.2 K4 N8 O24 Sb12 Zn2
• Calculated formula: C76.555 H146.2 K4 N8 O24 Sb12 Zn2
• Title of publication: [(ZnSb6)2]4-: a new structure type for coupled norbornadiene-like subunits
• Authors of publication: Wang, Yi; Zavalij, Peter Y.; Eichhorn, Bryan W.
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 32.346 ± 0.003 Å
• b: 14.3599 ± 0.0011 Å
• c: 26.819 ± 0.002 Å
• α: 90°
• β: 108.368 ± 0.0011°
• γ: 90°
• Cell volume: 11822.4 ± 1.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1166
• Residual factor for significantly intense reflections: 0.0652
• Weighted residual factors for significantly intense reflections: 0.1351
• Weighted residual factors for all reflections included in the refinement: 0.1568
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No