Information card for entry 7120779

Structure parameters

• Formula: C46 H101 Ce Cl O14.5 Si3
• Calculated formula: C46 H101 Ce Cl O14.5 Si3
• Title of publication: Synthesis and derivatisation of ceric tris(tert-butoxy)siloxides
• Authors of publication: Friedrich, Jochen; Maichle-moessmer, Caecilia; Anwander, Reiner
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 24.8822 ± 0.0013 Å
• b: 14.2617 ± 0.0008 Å
• c: 38.922 ± 0.002 Å
• α: 90°
• β: 107.382 ± 0.001°
• γ: 90°
• Cell volume: 13181.2 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0423
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0855
• Weighted residual factors for all reflections included in the refinement: 0.0883
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No