Information card for entry 7121023

Structure parameters

• Formula: C32 H39.5 Al2 Cl6 F0.5 N2 O2 P
• Calculated formula: C32 H39.5 Al2 Cl6 F0.5 N2 O2 P
• Title of publication: An imine-gallium Lewis pair stabilized oxophosphinidene via an unexpected phosphirene rearrangement.
• Authors of publication: Liu, Liu Leo; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 9
• Pages of publication: 1041 - 1044
• a: 10.578 ± 0.0006 Å
• b: 17.3535 ± 0.0009 Å
• c: 21.099 ± 0.001 Å
• α: 90°
• β: 96.898 ± 0.003°
• γ: 90°
• Cell volume: 3845 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.101
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for significantly intense reflections: 0.1391
• Weighted residual factors for all reflections included in the refinement: 0.1618
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No