Information card for entry 7121063

Structure parameters

• Chemical name: Dichloro-(1,4,7,10,13,16-hexaoxa-cyclononadec-18-ylmethyl)-phenylstannane bis(triphenylphosphine)iminium chloride complex
• Formula: C56.5 H63 Cl4 N O6 P2 Sn
• Calculated formula: C56.5 H63 Cl4 N O6 P2 Sn
• Title of publication: Interplay of Lewis acidity, intramolecular O→ Sn interactions and selectivity: organotin-functionalized crown ethers as ditopic hosts for sodium and potassium halides.
• Authors of publication: Tagne Kuate, Alain Charly; Naseer, Muhammad Moazzam; Lutter, Michael; Jurkschat, Klaus
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 7
• Pages of publication: 739 - 742
• a: 10.8696 ± 0.0008 Å
• b: 32.808 ± 0.003 Å
• c: 16.1991 ± 0.0013 Å
• α: 90°
• β: 95.866 ± 0.004°
• γ: 90°
• Cell volume: 5746.5 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1794
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1434
• Weighted residual factors for all reflections included in the refinement: 0.1971
• Goodness-of-fit parameter for all reflections included in the refinement: 0.831
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No