Information card for entry 7121098

Structure parameters

• Formula: C2 H12 B2 K N
• Calculated formula: C2 H12 B2 K N
• Title of publication: Dehydrogenation of dimethylamine-borane mediated by Group 1 pincer complexes.
• Authors of publication: Nolla-Saltiel, Roberto; Geer, Ana M.; Lewis, William; Blake, Alexander J.; Kays, Deborah L.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 15
• Pages of publication: 1825 - 1828
• a: 9.6343 ± 0.0003 Å
• b: 22.846 ± 0.0008 Å
• c: 13.1641 ± 0.0004 Å
• α: 90°
• β: 91.402 ± 0.003°
• γ: 90°
• Cell volume: 2896.62 ± 0.16 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1098
• Residual factor for significantly intense reflections: 0.0867
• Weighted residual factors for significantly intense reflections: 0.218
• Weighted residual factors for all reflections included in the refinement: 0.2395
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No