Information card for entry 7121146

Structure parameters

• Formula: C24 H62 Al Li N2 O3 Si4
• Calculated formula: C24 H62 Al Li N2 O3 Si4
• Title of publication: Lithium diamidodihydridoaluminates: bimetallic cooperativity in catalytic hydroboration and metallation applications
• Authors of publication: Pollard, Victoria A.; Orr, Samantha A.; McLellan, Ross; Kennedy, Alan R.; Hevia, Eva; Mulvey, Robert E.
• Journal of publication: Chemical Communications
• Year of publication: 2018
• a: 19.1211 ± 0.0007 Å
• b: 11.6571 ± 0.0005 Å
• c: 16.3906 ± 0.0006 Å
• α: 90°
• β: 90.154 ± 0.003°
• γ: 90°
• Cell volume: 3653.4 ± 0.2 ų
• Cell temperature: 151.4 K
• Ambient diffraction temperature: 151.4 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0801
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1181
• Weighted residual factors for all reflections included in the refinement: 0.1345
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No