Crystallography Open Database

Information card for entry 7121185

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Coordinates	7121185.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C292 H330 N24 O95 P8 Pd24
Calculated formula	C292 H330 N24 O95 P8 Pd24
Title of publication	Imido-P(v) trianion supported enantiopure neutral tetrahedral Pd(ii) cages.
Authors of publication	Rajasekar, Prabhakaran; Pandey, Swechchha; Paithankar, Harshad; Chugh, Jeetender; Steiner, Alexander; Boomishankar, Ramamoorthy
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	15
Pages of publication	1873 - 1876
a	20.679 ± 0.002 Å
b	25.531 ± 0.002 Å
c	31.458 ± 0.003 Å
α	90°
β	94.48 ± 0.002°
γ	90°
Cell volume	16558 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0755
Residual factor for significantly intense reflections	0.0689
Weighted residual factors for significantly intense reflections	0.1781
Weighted residual factors for all reflections included in the refinement	0.1837
Goodness-of-fit parameter for all reflections included in the refinement	1.133
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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