Information card for entry 7121346

Structure parameters

• Formula: C32 H23 B F4 N2
• Calculated formula: C32 H23 B F4 N2
• Title of publication: An umpolung of Lewis acidity/basicity at nitrogen by deprotonation of a cyclic (amino)(aryl)nitrenium cation.
• Authors of publication: Zhou, Jiliang; Liu, Liu Leo; Cao, Levy L.; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 35
• Pages of publication: 4390 - 4393
• a: 9.9397 ± 0.0016 Å
• b: 12.0611 ± 0.0019 Å
• c: 21.14 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2534.3 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.02 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for significantly intense reflections: 0.0725
• Weighted residual factors for all reflections included in the refinement: 0.0827
• Goodness-of-fit parameter for all reflections included in the refinement: 0.989
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No