Information card for entry 7121348

Structure parameters

• Formula: C32 H22 N2
• Calculated formula: C32 H22 N2
• Title of publication: An umpolung of Lewis acidity/basicity at nitrogen by deprotonation of a cyclic (amino)(aryl)nitrenium cation.
• Authors of publication: Zhou, Jiliang; Liu, Liu Leo; Cao, Levy L.; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 35
• Pages of publication: 4390 - 4393
• a: 13.2204 ± 0.0015 Å
• b: 10.9447 ± 0.0012 Å
• c: 17.0214 ± 0.0018 Å
• α: 90°
• β: 112.336 ± 0.003°
• γ: 90°
• Cell volume: 2278.1 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.074
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1302
• Weighted residual factors for all reflections included in the refinement: 0.1448
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No