Information card for entry 7121389

Structure parameters

• Chemical name: 4-methyl-2-nitro-5-tosyl-5,5a,6,10b-tetrahydroindeno[2,1-b]indole
• Formula: C23 H20 N2 O4 S
• Calculated formula: C23 H20 N2 O4 S
• Title of publication: Synthesis of indolines via a palladium/norbornene-catalyzed reaction of aziridines with aryl iodides.
• Authors of publication: Liu, Ce; Liang, Yujie; Zheng, Nian; Zhang, Bo-Sheng; Feng, Yuan; Bi, Siwei; Liang, Yong-Min
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 27
• Pages of publication: 3407 - 3410
• a: 12.0329 ± 0.0009 Å
• b: 24.1681 ± 0.0014 Å
• c: 8.5244 ± 0.0005 Å
• α: 90°
• β: 103.965 ± 0.007°
• γ: 90°
• Cell volume: 2405.7 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1344
• Residual factor for significantly intense reflections: 0.0621
• Weighted residual factors for significantly intense reflections: 0.1335
• Weighted residual factors for all reflections included in the refinement: 0.1645
• Goodness-of-fit parameter for all reflections included in the refinement: 0.902
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No