Information card for entry 7121394

Structure parameters

• Formula: C22 H4 O19 Os6
• Calculated formula: C22 H4 O19 Os6
• Title of publication: Multiple cluster CH activations and transformations of furan by triosmium carbonyl complexes.
• Authors of publication: Adams, Richard D.; Kiprotich, Emmanuel J.; Smith, Mark D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 28
• Pages of publication: 3464 - 3467
• a: 15.0941 ± 0.0012 Å
• b: 9.2362 ± 0.0007 Å
• c: 23.5146 ± 0.0018 Å
• α: 90°
• β: 103.717 ± 0.002°
• γ: 90°
• Cell volume: 3184.7 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.0953
• Weighted residual factors for all reflections included in the refinement: 0.1039
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No