Information card for entry 7121398

Structure parameters

• Formula: C22 H4 O19 Os6
• Calculated formula: C22 H4 O19 Os6
• Title of publication: Multiple cluster CH activations and transformations of furan by triosmium carbonyl complexes.
• Authors of publication: Adams, Richard D.; Kiprotich, Emmanuel J.; Smith, Mark D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 28
• Pages of publication: 3464 - 3467
• a: 9.7044 ± 0.0005 Å
• b: 11.2944 ± 0.0005 Å
• c: 15.7359 ± 0.0007 Å
• α: 82.9237 ± 0.0016°
• β: 86.2639 ± 0.0016°
• γ: 67.6042 ± 0.0015°
• Cell volume: 1582.19 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0444
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0467
• Weighted residual factors for all reflections included in the refinement: 0.0506
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No