Information card for entry 7121443

Structure parameters

• Formula: C32 H33 F6 Ge N7 O6 S2
• Calculated formula: C32 H33 F6 Ge N7 O6 S2
• Title of publication: Oxidation of a germanium(ii) dication to access cationic germanium(iv) fluorides.
• Authors of publication: Suter, Riccardo; Swidan, Ala'aeddeen; Macdonald, Charles L. B.; Burford, Neil
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 33
• Pages of publication: 4140 - 4143
• a: 14.7605 ± 0.0007 Å
• b: 11.2818 ± 0.0005 Å
• c: 21.5537 ± 0.001 Å
• α: 90°
• β: 96.184 ± 0.002°
• γ: 90°
• Cell volume: 3568.3 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.043
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for significantly intense reflections: 0.0798
• Weighted residual factors for all reflections included in the refinement: 0.0864
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0506
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No