Information card for entry 7121591
| Formula |
C70 H52 B F24 P Ru |
| Calculated formula |
C70 H52 B F24 P Ru |
| Title of publication |
P-C reductive elimination in Ru(ii) complexes to convert triarylphosphine ligands into five- or six-membered phosphacycles. |
| Authors of publication |
Kuwabara, Takuya; Kato, Takahiro; Takano, Kouichi; Kodama, Shintaro; Manabe, Yuuka; Tsuchida, Noriko; Takano, Keiko; Minami, Yasunori; Hiyama, Tamejiro; Ishii, Youichi |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2018 |
| Journal volume |
54 |
| Journal issue |
42 |
| Pages of publication |
5357 - 5360 |
| a |
17.512 ± 0.002 Å |
| b |
19.924 ± 0.003 Å |
| c |
21.061 ± 0.003 Å |
| α |
109.815 ± 0.0014° |
| β |
93.484 ± 0.0015° |
| γ |
110.481 ± 0.0013° |
| Cell volume |
6340.7 ± 1.5 Å3 |
| Cell temperature |
93 ± 2 K |
| Ambient diffraction temperature |
93 ± 2 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.108 |
| Residual factor for significantly intense reflections |
0.0687 |
| Weighted residual factors for significantly intense reflections |
0.1515 |
| Weighted residual factors for all reflections included in the refinement |
0.1771 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.066 |
| Diffraction radiation wavelength |
0.71075 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7121591.html
