Information card for entry 7121769

Structure parameters

• Formula: C19 H15 N O3 S
• Calculated formula: C19 H15 N O3 S
• Title of publication: Silver-copper co-catalyzed cascade intramolecular cyclization/desulfinamide/dehydrogenation: one-pot synthesis of substituted carbazoles.
• Authors of publication: Huang, Yuanqiong; Guo, Zhonglin; Song, Hongjian; Liu, Yuxiu; Wang, Qingmin
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 52
• Pages of publication: 7143 - 7146
• a: 17.529 ± 0.0004 Å
• b: 10.184 ± 0.0002 Å
• c: 18.2727 ± 0.0004 Å
• α: 90°
• β: 99.753 ± 0.002°
• γ: 90°
• Cell volume: 3214.81 ± 0.12 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.052
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.1065
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No