Information card for entry 7121790
| Formula |
C30 H27 N O4 |
| Calculated formula |
C30 H27 N O4 |
| Title of publication |
Phase-transfer-catalysed asymmetric synthesis of 2,2-disubstituted 1,4-benzoxazin-3-ones. |
| Authors of publication |
Pawliczek, Martin; Shimazaki, Yuto; Kimura, Hidenori; Oberg, Kevin M.; Zakpur, Saman; Hashimoto, Takuya; Maruoka, Keiji |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2018 |
| Journal volume |
54 |
| Journal issue |
51 |
| Pages of publication |
7078 - 7080 |
| a |
9.49079 ± 0.00017 Å |
| b |
9.73586 ± 0.00018 Å |
| c |
26.0784 ± 0.0005 Å |
| α |
90° |
| β |
90° |
| γ |
90° |
| Cell volume |
2409.67 ± 0.08 Å3 |
| Cell temperature |
123 K |
| Ambient diffraction temperature |
123 K |
| Number of distinct elements |
4 |
| Space group number |
19 |
| Hermann-Mauguin space group symbol |
P 21 21 21 |
| Hall space group symbol |
P 2ac 2ab |
| Residual factor for all reflections |
0.0401 |
| Residual factor for significantly intense reflections |
0.0363 |
| Weighted residual factors for significantly intense reflections |
0.1045 |
| Weighted residual factors for all reflections included in the refinement |
0.1086 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.893 |
| Diffraction radiation wavelength |
1.54187 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7121790.html
