Information card for entry 7121803

Structure parameters

• Formula: C57.5 H98 N3 O Si3 Y
• Calculated formula: C57.5 H98 N3 O Si3 Y
• Title of publication: Rare earth arylsilazido compounds with inequivalent secondary interactions.
• Authors of publication: Boteju, Kasuni C.; Wan, Suchen; Venkatesh, Amrit; Ellern, Arkady; Rossini, Aaron J.; Sadow, Aaron D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 53
• Pages of publication: 7318 - 7321
• a: 18.7125 ± 0.0003 Å
• b: 31.04 ± 0.0006 Å
• c: 20.6586 ± 0.0004 Å
• α: 90°
• β: 93.071 ± 0.001°
• γ: 90°
• Cell volume: 11982 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0542
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.0948
• Weighted residual factors for all reflections included in the refinement: 0.1041
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No