Information card for entry 7121972
| Formula |
C33 H63 B3 Cl3 N9 Si6 |
| Calculated formula |
C33 H63 B3 Cl3 N9 Si6 |
| Title of publication |
Group 13 element containing conformationally rigid "N-E-N" heteroatomic bridged [3.3](2,6)pyridinophanes (E = B, Al). |
| Authors of publication |
Bawari, Deependra; Negi, Chandrakala; Jaiswal, Kuldeep; Prashanth, Billa; Choudhury, Angshuman Roy; Singh, Sanjay |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2018 |
| Journal volume |
54 |
| Journal issue |
64 |
| Pages of publication |
8857 - 8860 |
| a |
11.3419 ± 0.0004 Å |
| b |
14.9551 ± 0.0005 Å |
| c |
16.2731 ± 0.0005 Å |
| α |
98.833 ± 0.001° |
| β |
110.206 ± 0.001° |
| γ |
102.878 ± 0.002° |
| Cell volume |
2443.71 ± 0.15 Å3 |
| Cell temperature |
100 ± 0.2 K |
| Ambient diffraction temperature |
100 ± 0.2 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.031 |
| Residual factor for significantly intense reflections |
0.0269 |
| Weighted residual factors for significantly intense reflections |
0.0707 |
| Weighted residual factors for all reflections included in the refinement |
0.0737 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.046 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7121972.html
