Information card for entry 7122085
| Chemical name |
(2R*,3R*)-N-Benzyl-2- ((S*)-1-hydroxy-3-phenylpropyl)-3-(trifluoromethyl)glutarimide |
| Formula |
C22 H22 F3 N O3 |
| Calculated formula |
C22 H22 F3 N O3 |
| Title of publication |
Stereoselective aldol reactions using pseudo C<sub>2</sub> symmetric 1-benzyl-4-(trifluoromethyl)piperidine-2,6-dione. |
| Authors of publication |
Inoue, Yuta; Hatayama, Takahiro; Kawasaki-Takasuka, Tomoko; Agou, Tomohiro; Kubota, Toshio; Yamazaki, Takashi |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2018 |
| Journal volume |
54 |
| Journal issue |
71 |
| Pages of publication |
9913 - 9916 |
| a |
9.8654 ± 0.0011 Å |
| b |
10.7372 ± 0.0012 Å |
| c |
11.1375 ± 0.0013 Å |
| α |
66.63 ± 0.005° |
| β |
79.912 ± 0.006° |
| γ |
63.756 ± 0.005° |
| Cell volume |
971.3 ± 0.2 Å3 |
| Cell temperature |
293 K |
| Ambient diffraction temperature |
293 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0514 |
| Residual factor for significantly intense reflections |
0.0415 |
| Weighted residual factors for significantly intense reflections |
0.0969 |
| Weighted residual factors for all reflections included in the refinement |
0.1031 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.025 |
| Diffraction radiation wavelength |
0.71075 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7122085.html
