Information card for entry 7122198

Structure parameters

• Formula: C25 H35 Cl3 O5 Si
• Calculated formula: C25 H35 Cl3 O5 Si
• Title of publication: Asymmetric total synthesis of pleurospiroketals A and B.
• Authors of publication: Kobayashi, Toyoharu; Tanaka, Konomi; Ishida, Masako; Yamakita, Natsumi; Abe, Hideki; Ito, Hisanaka
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 73
• Pages of publication: 10316 - 10319
• a: 8.2183 ± 0.0005 Å
• b: 12.5178 ± 0.0007 Å
• c: 28.0079 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2881.3 ± 0.3 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0335
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0613
• Weighted residual factors for all reflections included in the refinement: 0.0634
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No