Crystallography Open Database

Information card for entry 7122257

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Coordinates	7122257.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H28 O2 P2
Calculated formula	C29 H28 O2 P2
Title of publication	1,1-Diphosphines and divinylphosphines via base catalyzed hydrophosphination.
Authors of publication	Coles, N. T.; Mahon, M. F.; Webster, R. L.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	74
Pages of publication	10443 - 10446
a	9.8918 ± 0.0003 Å
b	11.8798 ± 0.0007 Å
c	12.5977 ± 0.0006 Å
α	117.242 ± 0.005°
β	103.91 ± 0.003°
γ	98.15 ± 0.004°
Cell volume	1221.99 ± 0.13 Å³
Cell temperature	150.03 ± 0.1 K
Ambient diffraction temperature	150.03 ± 0.1 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.039
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.0965
Weighted residual factors for all reflections included in the refinement	0.0989
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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