Information card for entry 7122287

Structure parameters

• Formula: C22 H35 F14 N O2 P4 W3
• Calculated formula: C22 H35 F14 N O2 P4 W3
• Title of publication: Neutral and cationic tungsten(vi) fluoride complexes with tertiary phosphine and arsine coordination.
• Authors of publication: Levason, William; Monzittu, Francesco M.; Reid, Gillian; Zhang, Wenjian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 83
• Pages of publication: 11681 - 11684
• a: 16.7303 ± 0.001 Å
• b: 17.878 ± 0.002 Å
• c: 24.095 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7206.9 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0678
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.0863
• Weighted residual factors for all reflections included in the refinement: 0.1013
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No