Crystallography Open Database

Information card for entry 7122434

Preview

Coordinates	7122434.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41.67 H53.67 B2 Cl2 N12 O4 P Si W2
Calculated formula	C41.6666 H53.6666 B2 Cl1.9998 N12 O4 P Si W2
Title of publication	Alkynylbis(alkylidynyl)phosphines: {L<sub>n</sub>M[triple bond, length as m-dash]C}<sub>2</sub>PC[triple bond, length as m-dash]CR.
Authors of publication	Frogley, Benjamin J.; Hill, Anthony F.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	87
Pages of publication	12373 - 12376
a	21.7758 ± 0.0004 Å
b	10.976 ± 0.0002 Å
c	24.157 ± 0.0008 Å
α	90°
β	115.485 ± 0.002°
γ	90°
Cell volume	5212 ± 0.2 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	9
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0419
Residual factor for significantly intense reflections	0.0389
Weighted residual factors for significantly intense reflections	0.1043
Weighted residual factors for all reflections included in the refinement	0.1076
Goodness-of-fit parameter for all reflections included in the refinement	1.103
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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