Crystallography Open Database

Information card for entry 7122452

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Coordinates	7122452.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H26 Br P
Calculated formula	C24 H26 Br P
Title of publication	A convenient route to internally phosphane-stabilized aryltriborane(7) compounds.
Authors of publication	Li, Jun; Daniliuc, Constantin G.; Kehr, Gerald; Erker, Gerhard
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	89
Pages of publication	12606 - 12609
a	7.9924 ± 0.0002 Å
b	15.6376 ± 0.0005 Å
c	33.0811 ± 0.0013 Å
α	90°
β	90°
γ	90°
Cell volume	4134.5 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0998
Residual factor for significantly intense reflections	0.0712
Weighted residual factors for significantly intense reflections	0.1291
Weighted residual factors for all reflections included in the refinement	0.146
Goodness-of-fit parameter for all reflections included in the refinement	1.13
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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