Information card for entry 7122481
| Formula |
C32 H28 N4 O2 |
| Calculated formula |
C32 H28 N4 O2 |
| Title of publication |
NaHS·nH<sub>2</sub>O-induced umpolung: the synthesis of 2-acyl-3-aminoindoles from aryl methyl ketones and 2-aminobenzonitriles. |
| Authors of publication |
Geng, Xiao; Wu, Xia; Wang, Can; Zhao, Peng; Zhou, You; Sun, Xuan; Wang, Ling-Jiao; Guan, Wen-Juan; Wu, Yan-Dong; Wu, An-Xin |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2018 |
| Journal volume |
54 |
| Journal issue |
90 |
| Pages of publication |
12730 - 12733 |
| a |
9.7923 ± 0.0013 Å |
| b |
17.627 ± 0.002 Å |
| c |
15.121 ± 0.002 Å |
| α |
90° |
| β |
91.028 ± 0.002° |
| γ |
90° |
| Cell volume |
2609.6 ± 0.6 Å3 |
| Cell temperature |
296 ± 2 K |
| Ambient diffraction temperature |
296 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
9 |
| Hermann-Mauguin space group symbol |
C 1 c 1 |
| Hall space group symbol |
C -2yc |
| Residual factor for all reflections |
0.0492 |
| Residual factor for significantly intense reflections |
0.0374 |
| Weighted residual factors for significantly intense reflections |
0.0883 |
| Weighted residual factors for all reflections included in the refinement |
0.0949 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.059 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7122481.html
