Information card for entry 7122483

Structure parameters

• Formula: C25 H23 N O4
• Calculated formula: C25 H23 N O4
• Title of publication: Oxidative coupling of enolates using memory of chirality: an original enantioselective synthesis of quaternary α-amino acid derivatives.
• Authors of publication: Mambrini, Antonin; Gori, Didier; Guillot, Régis; Kouklovsky, Cyrille; Alezra, Valérie
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 90
• Pages of publication: 12742 - 12745
• a: 52.223 ± 0.002 Å
• b: 15.6152 ± 0.0006 Å
• c: 7.4921 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6109.6 ± 0.4 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 4
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.1634
• Residual factor for significantly intense reflections: 0.0788
• Weighted residual factors for significantly intense reflections: 0.1485
• Weighted residual factors for all reflections included in the refinement: 0.1855
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No