Information card for entry 7122485

Structure parameters

• Chemical name: Organic
• Formula: C32 H27 N O2
• Calculated formula: C32 H27 N O2
• Title of publication: Intramolecular cycloaddition/rearrangement cascade from gold(iii)-catalysed reactions of propargyl aryldiazoesters with cinnamyl imines.
• Authors of publication: Qiu, Huang; Arman, Hadi; Hu, Wenhao; Doyle, Michael P.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 91
• Pages of publication: 12828 - 12831
• a: 18.041 ± 0.004 Å
• b: 12.292 ± 0.003 Å
• c: 11.066 ± 0.002 Å
• α: 90°
• β: 94.663 ± 0.003°
• γ: 90°
• Cell volume: 2445.9 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1294
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.0797
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No