Crystallography Open Database

Information card for entry 7122574

Preview

Coordinates	7122574.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39.2 H44.8 F4.8 N4.8 O4.8 S1.6 Si0.8
Calculated formula	C39.2 H44.8 F4.8 N4.8 O4.8 S1.6 Si0.8
Title of publication	Taming a silyldiium cation and its reactivity towards sodium phosphaethynolate.
Authors of publication	Hermannsdorfer, André; Stephan, Douglas W.; Driess, Matthias
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	96
Pages of publication	13523 - 13526
a	12.8682 ± 0.0001 Å
b	24.121 ± 0.0002 Å
c	17.041 ± 0.0002 Å
α	90°
β	97.415 ± 0.001°
γ	90°
Cell volume	5245.19 ± 0.09 Å³
Cell temperature	149.97 ± 0.11 K
Ambient diffraction temperature	149.97 ± 0.11 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0444
Residual factor for significantly intense reflections	0.0375
Weighted residual factors for significantly intense reflections	0.0946
Weighted residual factors for all reflections included in the refinement	0.1009
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7122574.html