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Information card for entry 7122629
Preview
Coordinates | 7122629.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H16 As4 K10 N16 O10 W6 |
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Calculated formula | C16 As4 K10 N16 O10 W6 |
Title of publication | From oxide to a new type of molecular tungsten compound: formation of bitetrahedral cluster complexes [{W<sub>6</sub>(μ<sub>4</sub>-O)<sub>2</sub>(μ<sub>3</sub>-CCN)<sub>4</sub>}(CN)<sub>16</sub>]<sup>10-</sup> and [{W<sub>6</sub>(μ<sub>4</sub>-O)<sub>2</sub>(μ<sub>3</sub>-As)<sub>4</sub>}(CN)<sub>16</sub>]<sup>10</sup>. |
Authors of publication | Yarovoy, Spartak S.; Smolentsev, Anton I.; Kozlova, Svetlana G.; Kompankov, Nikolay B.; Gayfulin, Yakov M.; Asanov, Igor P.; Yanshole, Vadim V.; Mironov, Yuri V. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2018 |
Journal volume | 54 |
Journal issue | 98 |
Pages of publication | 13837 - 13840 |
a | 11.844 ± 0.0003 Å |
b | 17.5913 ± 0.0004 Å |
c | 12.0559 ± 0.0003 Å |
α | 90° |
β | 107.084 ± 0.001° |
γ | 90° |
Cell volume | 2401.03 ± 0.1 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0459 |
Residual factor for significantly intense reflections | 0.0337 |
Weighted residual factors for significantly intense reflections | 0.0759 |
Weighted residual factors for all reflections included in the refinement | 0.0798 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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structural data.