Information card for entry 7122708

Structure parameters

• Formula: C68 H96 Eu I2 N4 O10
• Calculated formula: C68 H96 Eu I2 N4 O10
• Title of publication: Access to divalent lanthanide NHC complexes by redox-transmetallation from silver and CO2 insertion reactions
• Authors of publication: Simler, Thomas; Feuerstein, Thomas J.; Yadav, Ravi; Gamer, Michael T.; Roesky, Peter W.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 8.7081 ± 0.0006 Å
• b: 24.238 ± 0.003 Å
• c: 16.4401 ± 0.0012 Å
• α: 90°
• β: 100.78 ± 0.006°
• γ: 90°
• Cell volume: 3408.7 ± 0.5 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1514
• Residual factor for significantly intense reflections: 0.0864
• Weighted residual factors for significantly intense reflections: 0.2148
• Weighted residual factors for all reflections included in the refinement: 0.2802
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No