Information card for entry 7122809

Structure parameters

• Formula: C52.24 H46.48 Cl4.48 P4 Rh2
• Calculated formula: C52.2666 H46.5332 Cl4.5332 P4 Rh2
• Title of publication: Halogenation of A-Frame μ-Carbido Complexes: Synthesis of η2-Halocarbynes
• Authors of publication: Hill, Anthony; Barnett, Harrison J.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 21.268 ± 0.0004 Å
• b: 21.268 ± 0.0004 Å
• c: 14.3108 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6473.2 ± 0.2 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 76
• Hermann-Mauguin space group symbol: P 41
• Hall space group symbol: P 4w
• Residual factor for all reflections: 0.0833
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for significantly intense reflections: 0.1562
• Weighted residual factors for all reflections included in the refinement: 0.1815
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No