Information card for entry 7122887

Structure parameters

• Formula: C23 H22 N2
• Calculated formula: C23 H22 N2
• Title of publication: An Intramolecular C(sp3)−H Imination using PhI-mCPBA
• Authors of publication: Bose, Anima; Maiti, Saikat; Sau, Sudip; Mal, Prasenjit
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 9.3816 ± 0.0002 Å
• b: 10.7214 ± 0.0002 Å
• c: 11.0369 ± 0.0002 Å
• α: 106.328 ± 0.002°
• β: 109.83 ± 0.002°
• γ: 107.983 ± 0.002°
• Cell volume: 896.17 ± 0.04 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1075
• Residual factor for significantly intense reflections: 0.1
• Weighted residual factors for significantly intense reflections: 0.2774
• Weighted residual factors for all reflections included in the refinement: 0.2917
• Goodness-of-fit parameter for all reflections included in the refinement: 1.211
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No