Information card for entry 7122948

Structure parameters

• Formula: C49 H83 K N2 O7 U
• Calculated formula: C49 H83 K N2 O7 U
• Title of publication: Isolation of U(ii) compounds using strong donor ligands, C5Me4H and N(SiMe3)2, including a three-coordinate U(ii) complex
• Authors of publication: Ryan, Austin J.; Angadol, Mary A.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 30.199 ± 0.005 Å
• b: 13.568 ± 0.002 Å
• c: 30.609 ± 0.007 Å
• α: 90°
• β: 114.784 ± 0.0017°
• γ: 90°
• Cell volume: 11387 ± 4 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0582
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0795
• Weighted residual factors for all reflections included in the refinement: 0.0864
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No