Information card for entry 7123126

Structure parameters

• Formula: C37 H32 Au B F16 N O4 P S2 Si
• Calculated formula: C37 H32 Au B F16 N O4 P S2 Si
• Title of publication: Unsaturated Vicinal Frustrated Phosphane/Borane Lewis Pairs as Ligands in Gold(I) Chemistry
• Authors of publication: Ueno, Atsushi; Watanabe, Kohei; Daniliuc, Constantin Gabriel; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 39.0501 ± 0.0018 Å
• b: 10.3111 ± 0.0005 Å
• c: 23.3236 ± 0.0009 Å
• α: 90°
• β: 101.224 ± 0.001°
• γ: 90°
• Cell volume: 9211.6 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 10
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0335
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0538
• Weighted residual factors for all reflections included in the refinement: 0.0552
• Goodness-of-fit parameter for all reflections included in the refinement: 1.171
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No