Information card for entry 7123144

Structure parameters

• Formula: C21 H39 N O4 S Si
• Calculated formula: C21 H39 N O4 S Si
• Title of publication: Divergent synthesis of polysubstituted cyclopropanes and β-silyoxy imidates via switchable additions of N-tert-butanesulfinylimidates to acylsilanes
• Authors of publication: Tang, Fan; Ma, Peng-Ju; Yao, Yun; Xu, Yan-Jun; Lu, Chong-Dao
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.242 ± 0.0005 Å
• b: 6.4724 ± 0.0003 Å
• c: 14.3242 ± 0.0005 Å
• α: 90°
• β: 92.113 ± 0.003°
• γ: 90°
• Cell volume: 1226.86 ± 0.08 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0634
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.1695
• Weighted residual factors for all reflections included in the refinement: 0.1701
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No