Information card for entry 7123283

Structure parameters

• Formula: C75 H93 N O4 P3 S3 Si V
• Calculated formula: C75 H93 N O4 P3 S3 Si V
• Title of publication: Catalytic hydrazine disproportionation mediated by a thiolate-bridged VFe complex
• Authors of publication: Gu, Nina Xiao; Ung, Gaël; Peters, Jonas C.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 15.9471 ± 0.0008 Å
• b: 16.4072 ± 0.0008 Å
• c: 16.469 ± 0.0007 Å
• α: 117.261 ± 0.002°
• β: 102.796 ± 0.002°
• γ: 100.327 ± 0.002°
• Cell volume: 3534 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 99.99 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0773
• Residual factor for significantly intense reflections: 0.0543
• Weighted residual factors for significantly intense reflections: 0.1327
• Weighted residual factors for all reflections included in the refinement: 0.1455
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No