Information card for entry 7123367

Structure parameters

• Formula: C66 H86 Mn N4 O6 Sm
• Calculated formula: C66 H86 Mn N4 O6 Sm
• Title of publication: Rhenium is different: CO tetramerization induced by a divalent lanthanide complex in rhenium carbonyls
• Authors of publication: Yadav, Ravi; Simler, Thomas; Gamer, Michael T.; Köppe, Ralf; Roesky, Peter W.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 12.3657 ± 0.0003 Å
• b: 14.0273 ± 0.0003 Å
• c: 19.3568 ± 0.0005 Å
• α: 89.302 ± 0.002°
• β: 74.549 ± 0.002°
• γ: 78.249 ± 0.002°
• Cell volume: 3165.26 ± 0.14 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0489
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.084
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No