Crystallography Open Database

Information card for entry 7123378

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Coordinates	7123378.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H27 N Si
Calculated formula	C24 H27 N Si
Title of publication	PdCl2(CH3CN)2-catalyzed regioselective C-H olefinations of 2-amino biaryls with vinylsilanes as unactivated alkenes
Authors of publication	Sun, Qiao-Ying; Li, Zhao; Xu, Zheng; Zheng, Zhan-Jiang; Cao, Jian; Yang, Ke-Fang; Cui, Yu-Ming; Xu, Li-Wen
Journal of publication	Chemical Communications
Year of publication	2019
a	30.2149 ± 0.0014 Å
b	6.702 ± 0.0003 Å
c	23.0726 ± 0.001 Å
α	90°
β	113.218 ± 0.002°
γ	90°
Cell volume	4293.8 ± 0.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0988
Residual factor for significantly intense reflections	0.0529
Weighted residual factors for significantly intense reflections	0.1291
Weighted residual factors for all reflections included in the refinement	0.1542
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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