Aluminium-catalysed isocyanate trimerization, enhanced by exploiting a dynamic coordination sphere
Authors of publication
Bahili, Mohammed A.; Stokes, Emily C.; Amesbury, Robert C.; Ould, Darren M. C.; Christo, Bashar; Horne, Rhian J.; Kariuki, Benson M.; Stewart, Jack A.; Taylor, Rebekah L.; Williams, P. Andrew; Jones, Matthew D.; Harris, Kenneth D. M.; Ward, Benjamin D.
Journal of publication
Chemical Communications
Year of publication
2019
a
19.1233 ± 0.0013 Å
b
11.8499 ± 0.0008 Å
c
8.8509 ± 0.0006 Å
α
90°
β
108.543 ± 0.001°
γ
90°
Cell volume
1901.6 ± 0.2 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
9
Hermann-Mauguin space group symbol
C 1 c 1
Hall space group symbol
C -2yc
Residual factor for all reflections
0.0312
Residual factor for significantly intense reflections
0.0309
Weighted residual factors for significantly intense reflections
0.0784
Weighted residual factors for all reflections included in the refinement
0.0786
Goodness-of-fit parameter for all reflections included in the refinement
