Aluminium-catalysed isocyanate trimerization, enhanced by exploiting a dynamic coordination sphere
Authors of publication
Bahili, Mohammed A.; Stokes, Emily C.; Amesbury, Robert C.; Ould, Darren M. C.; Christo, Bashar; Horne, Rhian J.; Kariuki, Benson M.; Stewart, Jack A.; Taylor, Rebekah L.; Williams, P. Andrew; Jones, Matthew D.; Harris, Kenneth D. M.; Ward, Benjamin D.
Journal of publication
Chemical Communications
Year of publication
2019
a
13.5703 ± 0.0005 Å
b
11.6337 ± 0.0005 Å
c
14.6589 ± 0.0006 Å
α
90°
β
98.895 ± 0.004°
γ
90°
Cell volume
2286.41 ± 0.16 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0703
Residual factor for significantly intense reflections
0.0468
Weighted residual factors for significantly intense reflections
0.1055
Weighted residual factors for all reflections included in the refinement
0.1233
Goodness-of-fit parameter for all reflections included in the refinement
