Aluminium-catalysed isocyanate trimerization, enhanced by exploiting a dynamic coordination sphere
Authors of publication
Bahili, Mohammed A.; Stokes, Emily C.; Amesbury, Robert C.; Ould, Darren M. C.; Christo, Bashar; Horne, Rhian J.; Kariuki, Benson M.; Stewart, Jack A.; Taylor, Rebekah L.; Williams, P. Andrew; Jones, Matthew D.; Harris, Kenneth D. M.; Ward, Benjamin D.
Journal of publication
Chemical Communications
Year of publication
2019
a
23.3812 ± 0.0016 Å
b
37.1191 ± 0.0018 Å
c
7.722 ± 0.0005 Å
α
90°
β
90°
γ
90°
Cell volume
6701.8 ± 0.7 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
43
Hermann-Mauguin space group symbol
F d d 2
Hall space group symbol
F 2 -2d
Residual factor for all reflections
0.0521
Residual factor for significantly intense reflections
0.0419
Weighted residual factors for significantly intense reflections
0.0972
Weighted residual factors for all reflections included in the refinement
0.1046
Goodness-of-fit parameter for all reflections included in the refinement
