Crystallography Open Database

Information card for entry 7123761

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Coordinates	7123761.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H50 B2 O14 Si8
Calculated formula	C60 H50 B2 O14 Si8
Title of publication	A General Diversity Oriented Synthesis of Asymmetric Double-Decker Shaped Silsesquioxanes
Authors of publication	Barry, Badru-Deen; Dannatt, Jonathan Elvin; King, Austin Kendall; Lee, Andre; Maleczka, Robert
Journal of publication	Chemical Communications
Year of publication	2019
a	13.0387 ± 0.0009 Å
b	13.2083 ± 0.0009 Å
c	19.4033 ± 0.0014 Å
α	76.749 ± 0.001°
β	78.484 ± 0.001°
γ	68.265 ± 0.001°
Cell volume	2997 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0961
Residual factor for significantly intense reflections	0.0594
Weighted residual factors for significantly intense reflections	0.1444
Weighted residual factors for all reflections included in the refinement	0.1728
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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