Crystallography Open Database

Information card for entry 7123763

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Structure parameters

Formula	C62 H54 B2 O16 Si8
Calculated formula	C62 H54 B2 O16 Si8
Title of publication	A General Diversity Oriented Synthesis of Asymmetric Double-Decker Shaped Silsesquioxanes
Authors of publication	Barry, Badru-Deen; Dannatt, Jonathan Elvin; King, Austin Kendall; Lee, Andre; Maleczka, Robert
Journal of publication	Chemical Communications
Year of publication	2019
a	24.7461 ± 0.0003 Å
b	22.7525 ± 0.0004 Å
c	11.4396 ± 0.0002 Å
α	90°
β	93.626 ± 0.001°
γ	90°
Cell volume	6428.01 ± 0.18 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1208
Residual factor for significantly intense reflections	0.0577
Weighted residual factors for significantly intense reflections	0.1213
Weighted residual factors for all reflections included in the refinement	0.149
Goodness-of-fit parameter for all reflections included in the refinement	0.985
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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