Information card for entry 7123861

Structure parameters

• Formula: C35 H64 Cl Fe Ge N5 O3 Si2 Sn
• Calculated formula: C35 H64 Cl Fe Ge N5 O3 Si2 Sn
• Title of publication: Symmetric and non-symmetric bis-metallylene iron complexes, precursors of iron germanide nanoparticles
• Authors of publication: Sodreau, Alexandre; Lentz, Nicolas; Frutos, Maria; Ladeira, Sonia; Nayral, Celine; Delpech, Fabien; Madec, David
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 10.8967 ± 0.0004 Å
• b: 33.0836 ± 0.0013 Å
• c: 13.0091 ± 0.0006 Å
• α: 90°
• β: 105.207 ± 0.002°
• γ: 90°
• Cell volume: 4525.6 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 9
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.0538
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1047
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No