Information card for entry 7123868

Structure parameters

• Formula: C48 H54 As2 Ge N2
• Calculated formula: C48 H54 As2 Ge N2
• Title of publication: Reaction of an arsinoamide with chloro tetrylenes: substitution and As–N bond insertion
• Authors of publication: Chen, Xiao; Simler, Thomas; Yadav, Ravi; Gamer, Michael T.; Köppe, Ralf; Roesky, Peter W.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.0143 ± 0.0007 Å
• b: 18.0257 ± 0.0007 Å
• c: 19.1618 ± 0.001 Å
• α: 90°
• β: 107.787 ± 0.004°
• γ: 90°
• Cell volume: 4280.3 ± 0.4 ų
• Cell temperature: 210 K
• Ambient diffraction temperature: 210 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0629
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1053
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No