Information card for entry 7123880

Structure parameters

• Formula: C32 H36 Cl Cr P
• Calculated formula: C32 H36 Cl Cr P
• Title of publication: Synthesis and reactivity of asymmetric Cr(I) dinitrogen complexes supported by cyclopentadienyl-phosphine ligands
• Authors of publication: Li, Jiapeng; Yin, Jianhao; Wang, Gao-Xiang; Yin, Zhu-Bao; Zhang, Wen-Xiong; Xi, Zhenfeng
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 10.4291 ± 0.0003 Å
• b: 12.2337 ± 0.0003 Å
• c: 13.0486 ± 0.0005 Å
• α: 65.497 ± 0.003°
• β: 71.852 ± 0.003°
• γ: 73.717 ± 0.003°
• Cell volume: 1417.35 ± 0.09 ų
• Cell temperature: 179.98 ± 0.1 K
• Ambient diffraction temperature: 179.98 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0337
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0781
• Weighted residual factors for all reflections included in the refinement: 0.0805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No