Information card for entry 7123883

Structure parameters

• Formula: C128 H144 K4 P4
• Calculated formula: C128 H144 K4 P4
• Title of publication: Synthesis and reactivity of asymmetric Cr(I) dinitrogen complexes supported by cyclopentadienyl-phosphine ligands
• Authors of publication: Li, Jiapeng; Yin, Jianhao; Wang, Gao-Xiang; Yin, Zhu-Bao; Zhang, Wen-Xiong; Xi, Zhenfeng
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 17.9093 ± 0.0006 Å
• b: 18.1403 ± 0.0008 Å
• c: 20.5737 ± 0.0007 Å
• α: 113.944 ± 0.004°
• β: 100.357 ± 0.003°
• γ: 108.053 ± 0.003°
• Cell volume: 5437.1 ± 0.5 ų
• Cell temperature: 89.9 ± 0.5 K
• Ambient diffraction temperature: 89.9 ± 0.5 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1156
• Residual factor for significantly intense reflections: 0.0746
• Weighted residual factors for significantly intense reflections: 0.1738
• Weighted residual factors for all reflections included in the refinement: 0.1926
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No