Information card for entry 7123980

Structure parameters

• Formula: C75 H71 B Cl D3 F15 N4 P2
• Calculated formula: C75 H71 B Cl D3 F15 N4 P2
• Title of publication: Heteroleptic diphosphenes and arsaphosphenes bearing neutral and anionic N-heterocyclic carbenes
• Authors of publication: Ho, Luong Phong; Zaretzke, Marc-Kevin; Bannenberg, Thomas; Tamm, Matthias
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.545 ± 0.0006 Å
• b: 14.376 ± 0.001 Å
• c: 19.5043 ± 0.0008 Å
• α: 99.475 ± 0.004°
• β: 93.788 ± 0.004°
• γ: 109.582 ± 0.004°
• Cell volume: 3499.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0773
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1521
• Weighted residual factors for all reflections included in the refinement: 0.1668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No