Information card for entry 7124291

Structure parameters

• Formula: C21 H33 Au Cl O2 P3 Si3
• Calculated formula: C21 H33 Au Cl O2 P3 Si3
• Title of publication: Four Consecutive Reactions in one Pot: Cascade Formation of an Unprecedented Triphosphatricyclo[3.2.1.02,7]oct-3-ene
• Authors of publication: Giese, Steven; Buzsaki, Daniel; Nyulaszi, Laszlo; Muller, Christian
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.2862 ± 0.0018 Å
• b: 11.6119 ± 0.0014 Å
• c: 19.29 ± 0.003 Å
• α: 90°
• β: 98.741 ± 0.005°
• γ: 90°
• Cell volume: 2941.5 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.019
• Residual factor for significantly intense reflections: 0.0169
• Weighted residual factors for significantly intense reflections: 0.0411
• Weighted residual factors for all reflections included in the refinement: 0.0415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.096
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No