Information card for entry 7124293

Structure parameters

• Formula: C21 H33 O2 P3 Si3
• Calculated formula: C21 H33 O2 P3 Si3
• Title of publication: Four Consecutive Reactions in one Pot: Cascade Formation of an Unprecedented Triphosphatricyclo[3.2.1.02,7]oct-3-ene
• Authors of publication: Giese, Steven; Buzsaki, Daniel; Nyulaszi, Laszlo; Muller, Christian
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 8.941 ± 0.003 Å
• b: 9.608 ± 0.004 Å
• c: 16.384 ± 0.006 Å
• α: 106.21 ± 0.008°
• β: 103.338 ± 0.015°
• γ: 93.876 ± 0.01°
• Cell volume: 1301.9 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0343
• Residual factor for significantly intense reflections: 0.0273
• Weighted residual factors for significantly intense reflections: 0.062
• Weighted residual factors for all reflections included in the refinement: 0.0647
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No